Microbeam characterization of corning archeological reference glasses: New additions to the Smithsonian Microbeam Standard collection

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Microbeam Characterization of Corning Archeological Reference Glasses: New Additions to the Smithsonian Microbeam Standard Collection

An initial study of the minor element, trace element, and impurities in Corning archeological references glasses have been performed using three microbeam techniques: electron probe microanalysis (EPMA), laser ablation ICP-mass spectrometry (LA ICP-MS), and secondary ion mass spectrometry (SIMS). The EPMA results suggest a significant level of heterogeneity for a number of metals. Conversely, h...

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Smithsonian Microbeam Standards

This is a short history of the Smithsonian Microbeam Standards; their sources, selection, preparation, and analyses. Fifty-eight minerals, natural glasses, and synthetic samples have been characterized in the past 25 years. During that time, over 750 requests were received for approximately 11 000 individual samples. These reference samples are referred to as the Smithsonian Microbeam Standards.

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Critical assessment of the elemental composition of Corning archeological reference glasses by LA-ICP-MS

Corning archeological reference glasses A, B, C, and D have been made to simulate different historic technologies of glass production and are used as standards in historic glass investigations. In this work, nanoseconds (193, 266 nm) and femtosecond (800 nm) laser ablation were used to study the elemental composition of Corning glasses using laser ablation inductively coupled plasma mass spectr...

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Characterization of Corning EPMA Standard Glasses 95IRV, 95IRW, and 95IRX

The preparation, synthesis, and characterization of Corning trace-element glasses 95IRV, 95IRW, and 95IRX by bulk chemical and electron microprobe techniques is discussed. Working values for the doped elements in the 95-series glasses are established. Blank values have been determined by both bulk chemical and electron microprobe analysis, and important x-ray interferences are highlighted. Chem...

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ژورنال

عنوان ژورنال: Journal of Research of the National Institute of Standards and Technology

سال: 2002

ISSN: 1044-677X

DOI: 10.6028/jres.107.058